Tin Dioxide Nanostructure Using Rapid Thermal Oxidation Method and Hydrothermal Synthesis of CuO-SnO2-ZnO Nano Composite Oxides
[1]
Marwa Abdul Muhsien Hassan, Department of Physics, College of Science, Al- Mustansiriyah University, Baghdad, Iraq.
[2]
Evan Tareq Salem, School of Applied Sciences, University of Technology, Laser and Optoelectronic Branch, Baghdad, Iraq.
[3]
Nadheer Jassim Mohammed, Department of Physics, College of Science, Al- Mustansiriyah University, Baghdad, Iraq.
[4]
Ibrahim Ramdan Agool, Department of Physics, College of Science, Al- Mustansiriyah University, Baghdad, Iraq.
Tin dioxide (SnO2) nanostructured thin films on quartz substrates were prepared by rapid thermal oxidation technique for different oxidation temperatures and oxidation times. X-ray diffraction analysis indicates that the films are polycrystalline, having tetragonal structure. All the films shown most preferred orientation along (101) plane parallel to the substrates. The nanostructure parameters such as grain size, microstrain and dislocation density were calculated. The grain size of prepared SnO2 nanostructure films is small and is within the range of 44 to 56 nm. The nanocomposite oxides (CuO-SnO2-ZnO) prepared to use hydrothermal method consist of small nanorod distributed on the surface that shows nanostructure properties
SnO2 Polycrystalline Film, Rapid Thermal Oxidation, Structural Properties, Grain Size, Hydrothermal Method
[1]
T. J. Stanimirova, P. A. Atanasov, I. G. Dimitrov, A. O. Dikovska" Investigation on the structural and optical properties of tin oxide films grown by pulsed laser deposition" Journal of Optoelectronics and Advanced Materials, Vol. 7, No. 3, June (2005), pp: 1335 – 1340.
[2]
Novinrooz, Abdoljavad; Sarabadani, Parvin; Garousi, Javad "Characterization of Pure and Antimony Doped SnO2 Thin Films Prepared by the Sol-Gel Technique" Iran. J. Chem. Chem. Eng. Vol. 25, No.2, (2006), PP: 31-38.
[3]
Shengyue Wang, Wei Wang, Qingxiang Hu, Yitai Qian, "Surface modification of tin oxide ultrafine particle thin films", Materials Research Bulletin, Vol. 35, (2000), pp: 1235–1241.
[4]
Sardar M. Ayub Durrani "Biasing Voltage Dependence of Sensitivity of Electron Beam Evaporated SnO2 Thin Film CO Sensor" Sensors, Vol.6, (2006), pp: 1153-1160.
[5]
K. Zakrzewskaa, M. Radeckaa, J. Przewoz´nika, K. Kowalskia, P. Czuba "Microstructure and photoelectrochemical characterization of the TiO2–SnO2 system" Thin Solid Films, 490, (2005), pp: 101 – 107.
[6]
Young-ll Kim, Joo-Byoung Yoon, Jin-Ho Choy, Guy Campet, Didier Camino, Josik Portier, and Jean Salardenne" Rf sputtered SnO2, Sn-doped In2O3 and Ce-doped TiO2 films as transparent counter electrodes for electrochromic window" Bull. Korean Chem. Soc. Vol. 19, No. 1, (1998), pp: 107-109.
[7]
Divya Haridas, Arijit Chowdhuri, K. Sreenivas, and Vinay Gupta " Enhanced LPG response characteristics of SnO2 thin film based sensors loaded with Pt clusters" International journal on smart sensing and intelligent systems, Vol. 2, No. 3, (2009), pp: 503-514.
[8]
Jeong-Hoon Leea, Gun-Eik Janga, Dae-Ho Yoonb and Sang-Hee Sonc "Effect of deposition temperature on electro-optical properties of SnO2 thin films fabricated by a PECVD method" Journal of Ceramic Processing Research. Vol. 8, No. 1, (2007), pp: 59-63.
[9]
U. Pal, A. Pérez-Centeno, and M. Herrera-Zaldívar "Cathodoluminescence defect characterization of hydrothermally grown SnO2 nanoparticles" J. Appl. Phys. Vol. 103, No. 064301, (2008), pp: 1-6.
[10]
R.G. Dhere, H.R. Moutinho, S. Asher, D. Young, X. Li, R. Ribelin, and T. Gessert" Characterization of SnO2 Films Prepared Using Tin Tetrachloride and Tetra Methyl Tin Precursors" National Renewable Energy Laboratory, October (1998), pp: 1-6.
[11]
D.M. Qu, P.X. Yan, J.B. Chang, D. Yan, J.Z. Liu, G.H. Yue, R.F. Zhuo, H.T. Feng" Nanowires and nanowire–nanosheet junctions of SnO2 nanostructures" Materials Letters, Vol.61, (2007), pp: 2255–2258.
[12]
J. E. Dominguez, X. Q. Pan, L. Fu, P. A. Van Rompay, Z. Zhang, J. A. Nees, and P. P. Pronko, " Epitaxial SnO2 thin films grown on .1¯ 012. sapphire by femtosecond pulsed laser deposition", J. Appl. Phys., Vol. 91, No. 3, 1 February (2002), pp: 1060-1065.
[13]
J. E. Dominguez, L. Fu, and X. Q. Pan "Effect of crystal defects on the electrical properties in epitaxial tin dioxide thin films" Appl. Phys. Lett., Vol. 81, No. 27, 30 December (2002), pp: 5163-5170.
[14]
Jochan Joseph, Varghese Mathew, Jacob Mathew, K. E. Abraham " Studies on physical properties and carrier conversion of SnO2: Nd thin films" Turk J Phys, Vol. 33, (2008), pp: 37-47.
[15]
J. Geurts. S. Rau. W. Richter and F. J. Schmitte "SnO films and their oxidation to SnO2: Raman scattering. IR reflectivity and X-Ray diffraction" Thin Solid Films, (1984).
[16]
G. Gordillo; L. C. Moreno; W. De La Cruz; P.Teheran "Preparation and characterization of SnO2 thin films deposited by spray pyrolysis from SnCl2 and SnCl4 precursors" Thin Solid Films, Vol. 252, No. 1, (1994), pp: 61-66.
[17]
Yong-Sahm Choe, Jae-Ho Chung, Dae-Seung Kim, Gyeung-Ho Kim and Hong Koo Baik "Phase transformation and morphological evolution of ion-beam sputtered tin oxide films on silicon substrate" Materials Research Bulletin, Vol. 34, Issue 9, (1999), pp:1473-1479.
[18]
Brian S. Mitchell "An introduction to materials engineering and science for chemical and materials engineers" A John Wily & Sons, Inc., Hoboken, New Jersey. All rights reserved. Published simultaneously in Canada, (2004), pp: 43.
[19]
S. Mosadegh Sedghi, and M. Vesali Naseh "Sonochemically prepared SnO2 quantum dots as a selective and low temperature Co sensor" Proceedings of World Academy of Science, Engineering and Technology, Vol. 37, Issue 2070-3740, (2009).
[20]
L.V. Azarooff "Elementary of X-Ray Crystallography" Mc Graw-Hill Book Company, (1968), pp: 552-556.
[21]
Th. H. De. Keijser, J. Appl. Cryst., Vol.15, (1982), pp: 308-314.
[22]
A. Moses Ezhi Raj, L. C. Nehru, M. Jayachandran, and C. Sanjeeviraja "Spray pyrolysis deposition and characterization of highly (100) oriented magnesium oxide thin films" Cryst. Res. Technol.Vol. 42, No.9, (2007), pp: 867 – 875.
[23]
A.S. Edelestein, R.C. Camarata "Nanomaterials: Synthesis, Properties and Application, Institute of Physics" Publ., Bristol, UK, (1996).
[24]
Ali Jasim AL-Jabiry, " Studying the Effect of Molarity on the Physical and Sensing Properties of Zinc Oxide Thin Films Prepared by Spray Pyrolysis Technique" Phd (University of Technology), (2007), pp: .