Synthesis of Colloidal SnO2:Bi2O3 Nanoparticles Using Nanosecond Laser Ablation under Liquid
[1]
Mohammed Jawad Kadhim, Physics department, College of Sciences, Al-Mustansiriya University, Baghdad, 00964, Iraq.
[2]
Firas Sabeeh Mohammed, Physics department, College of Sciences, Al-Mustansiriya University, Baghdad, 00964, Iraq.
[3]
Marwa Abdul Muhsien Hassa, Physics department, College of Sciences, Al-Mustansiriya University, Baghdad, 00964, Iraq.
SnO2:Bi2O3 collodial NPs were synthesized by pulsed laser ablation of Sn:Bi target (50%:50%) in double distilled water (DDW) at room temperature. High purity Sn:Bi target (purity of 99.99%) was fixed at bottom of open a plastic cell containing of 2 ml DDW and DDW+ PVP which represent the liquid media. Ablation is carried out with laser operating at 1.064 nm wavelengths at fluence set in the range of 40.5J/cm2 and (60 laser pulses). The diffraction peaks in the XRD pattern broadened due to the particles in the sample are too small. The primary particle size calculated by Sherrer formula is about 20 nm. The spherical nanoparticles morphologies were carried out by scan electron microscope (SEM) analysis, exhibits spherical with average size distribution found to be 25 nm.
Nanoparticles, SnO2, PL, Laser Ablation, Bi2O3
[1]
Evan T. Salem, " Tin Oxide Nanoparticles Prepared Using Liquid Phase Laser Ablation for Optoelectronic Application", Nanoscience and Nanotechnology 2012, 2(3): 86-89 DOI: 10.5923/j.nn.20120203.08.
[2]
Luhua Jiang, Gongquan Sun, Zhenhua Zhou, Shiguo Sun, Qi Wang, Shiyou Yan, Huanqiao Li, Juan Tian, Junsong Guo, Bing Zhou, and Qin Xin, " Size-Controllable Synthesis of Monodispersed SnO2 Nanoparticles and Application in Electrocatalysts", J. Phys. Chem. B 2005, 109, 8774-8778.
[3]
A. J. Salazar-Pérez, M. A. Camacho-López, R. A. Morales-Luckie, V. Sánchez-Mendieta, F. Ureña-Núñez, J. Arenas-Alatorre, " Structural evolution of Bi2O3 prepared by thermal oxidation of bismuth nano-particles", Superficies y Vacío 18(3), 4-8, septiembre de 2005 ©Sociedad Mexicana de Ciencia y Tecnología de Superficies y Materiales.
[4]
Arun Prakash Periasamy, Singying Yang, Shen-Ming Chen, " Preparation and characterization of bismuth oxide nanoparticles-multiwalled carbon nanotube composite for the development of horseradish peroxidase based H2O2 biosensor", Talanta 87 (2011) 15– 23.
[5]
R.K. Swarnkar, S.C. Singh and R. Gopal, " OPTICAL CHARACTERIZATIONS OF COPPER OXIDE NANOMATERIAL", ICOP 2009-International Conference on Optics and Photonics CSIO, Chandigarh, India, 30 Oct.-1 Nov. 2009.
[6]
M. H. Shahrokh Abadi, M. N. Hamidon, Abdul Halim Shaari, Norhafizah Abdullah, Norhisam Misron and Rahman Wagiran," Characterization of Mixed xWO3(1-x)Y2O3 Nanoparticle Thick Film for Gas Sensing Application", Sensors 2010, 10, 5074-5089; doi:10.3390/s100505074.
[7]
Abdulrahman Khalaf Ali, "Preparation of Ag and Au Nanoparticles by Pulsed Laser Ablation in Liquids", phd thesis, 2010, Iraq.